Annual Progress Rpt - Fuel Element development [1962] - download pdf or read online

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006 A s Polished 520 x Figure 18 Microstructure o f 42 w/o U02 i n A1 Cermet, Heat Treated 40 Hours a t 1110" F. 8 w/o UO2 i n A1 Cermet, I r r a d i a t e d t o 30% Burnup. 006 A As Polished 500 x Figure 20 Microstructure of 24 w/o U 0 2 in A1 Cermet, Irradiated to M-716 8-17 45% Burnup. 8 w/o U02 i n A 1 Cermet, Irradiated to 40% Burnup. 006 A s Polished 500 x F i g u r e 22 M i c r o s t r u c t u r e of 24 w/o U02 i n A l Cermet, I r r a d i a t e d t o 18% Burnup a t 425°F. 7 w/o U02 i n A1 Cermet, I r r a d i a t e d t o 29% Burnup and P o s t - I r r a d i a t i o n A n r e d e d a t 390°F f o r 2 Hours.

This suggests some d i f f u s i o n c o n t r o l l e d r e a c t i o n between t h e U02 and aluminum. " P l a s t i c r e p l i c a s of t h e i r r a d i a t e d and u n i r r a d i a t e d samples were taken i n b o t h t h e a s - p o l i s h e d and etched c o n d i t i o n s . A l l of t h e s e r e p l i c a s were shadowed with platinum i n a vacuum evaporator and carbon was d e p o s i t e d normally onto t h e shadowed s u r f a c e s . The composite r e p l i c a s were c u t i n t o a p p r o p r i a t e l y s i z e d p i e c e s , mounted on specimen screens, and t h e p l a s t i c d i s s o l v e d away l e a v i n g a shadowed carbon r e p l i c a .

The inner layer, which is harder than the UO2 sinze'it appeared raised with respect to the U02 in the as-polished condition, is probably A1203. (ll) It is observed when burnup on the order of 50 a/o of the uranium are achieved. This rim has never been identified but may result from segregation of fission-product oxides out of the U02. , the U02 particles appear to have been liquid. The irradiation temperatures for the U02-A1 dispersions were low, x 300°F. " 3. Gamma Scanning of Fuel Plates It has long been of interest to determine just how closely the fuel burnout f o l l o w e d the vertical neutron f l u x distribution measured by flux wires in the water channels between the fuel plates.

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Annual Progress Rpt - Fuel Element development [1962]

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